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Nanoindentation creep testing: Advantages and limitations of the constant contact pressure method

Minnert, Christian ; Durst, Karsten (2024)
Nanoindentation creep testing: Advantages and limitations of the constant contact pressure method.
In: Journal of Materials Research, 2022, 37 (2)
doi: 10.26083/tuprints-00023578
Article, Secondary publication, Publisher's Version

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Item Type: Article
Type of entry: Secondary publication
Title: Nanoindentation creep testing: Advantages and limitations of the constant contact pressure method
Language: English
Date: 24 September 2024
Place of Publication: Darmstadt
Year of primary publication: 2022
Place of primary publication: Berlin
Publisher: Springer International Publishing
Journal or Publication Title: Journal of Materials Research
Volume of the journal: 37
Issue Number: 2
DOI: 10.26083/tuprints-00023578
Corresponding Links:
Origin: Secondary publication DeepGreen
Abstract:

Different loading protocols have been developed in the past to investigate the creep properties of materials using instrumented indentation testing technique. Recently, a new indentation creep method was presented, in which the contact pressure is kept constant during the creep test segment, similar to the constant stress applied in a uniaxial creep experiment. In this study, the results of constant contact pressure creep tests are compared to uniaxial and constant load hold indentation creep experiments on ultrafine grained Cu and CuAl5. The constant contact pressure method yields similar stress exponents as the uniaxial tests, down to indentation strain rates of 10⁻⁶ s⁻¹, whereas the constant load hold method results mainly in a relaxation of the material at decreasing applied pressures. Furthermore, a pronounced change in the power law exponent at large stress reductions is found for both uniaxial and constant contact pressure tests, indicating a change in deformation mechanism of ultrafine grained metals.

Uncontrolled Keywords: Nanoindentation, Creep, Strain rate sensitivity, Severe plastic deformation, Ultrafine grained microstructure, Copper alloys
Status: Publisher's Version
URN: urn:nbn:de:tuda-tuprints-235789
Classification DDC: 500 Science and mathematics > 530 Physics
500 Science and mathematics > 540 Chemistry
Divisions: 11 Department of Materials and Earth Sciences > Material Science > Physical Metallurgy
Date Deposited: 24 Sep 2024 09:32
Last Modified: 21 Oct 2024 07:55
SWORD Depositor: Deep Green
URI: https://tuprints.ulb.tu-darmstadt.de/id/eprint/23578
PPN: 522322492
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