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  5. Flexible Sample Environment for the Investigation of Soft Matter at the European Spallation Source: Part II—The GISANS Setup
 
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2021
Zweitveröffentlichung
Artikel
Verlagsversion

Flexible Sample Environment for the Investigation of Soft Matter at the European Spallation Source: Part II—The GISANS Setup

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Hauptpublikation
applsci-11-04036-v2 (1).pdf
CC BY 4.0 International
Format: Adobe PDF
Size: 5.53 MB
TUDa URI
tuda/7365
URN
urn:nbn:de:tuda-tuprints-193886
DOI
10.26083/tuprints-00019388
Autor:innen
Widmann, Tobias ORCID 0000-0002-1656-1852
Kreuzer, Lucas P. ORCID 0000-0002-9669-2130
Kühnhammer, Matthias ORCID 0000-0002-8377-2772
Schmid, Andreas J. ORCID 0000-0002-4205-0861
Wiehemeier, Lars ORCID 0000-0002-8827-6807
Jaksch, Sebastian ORCID 0000-0001-5358-8651
Frielinghaus, Henrich ORCID 0000-0002-8812-8783
Löhmann, Oliver ORCID 0000-0002-1527-1319
Schneider, Harald
Hiess, Arno ORCID 0000-0002-6457-691X
Klitzing, Regine von ORCID 0000-0003-0555-5104
Hellweg, Thomas ORCID 0000-0002-2394-5846
Müller-Buschbaum, Peter ORCID 0000-0002-9566-6088
Kurzbeschreibung (Abstract)

The FlexiProb project is a joint effort of three soft matter groups at the Universities of Bielefeld, Darmstadt, and Munich with scientific support from the European Spallation Source (ESS), the small-K advanced diffractometer (SKADI) beamline development group of the Jülich Centre for Neutron Science (JCNS), and the Heinz Maier-Leibnitz Zentrum (MLZ).Within this framework, a flexible and quickly interchangeable sample carrier system for small-angle neutron scattering (SANS) at the ESS was developed. In the present contribution, the development of a sample environment for the investigation of soft matter thin films with grazing-incidence small-angle neutron scattering (GISANS) is introduced. Therefore, components were assembled on an optical breadboard for the measurement of thin film samples under controlled ambient conditions, with adjustable temperature and humidity, as well as the optional in situ recording of the film thickness via spectral reflectance. Samples were placed in a 3D-printed spherical humidity metal chamber, which enabled the accurate control of experimental conditions via water-heated channels within its walls. A separately heated gas flow stream supplied an adjustable flow of dry or saturated solvent vapor. First test experiments proved the concept of the setup and respective component functionality.

Freie Schlagworte

GISANS

sample environment

3D printed

humidity chamber

thin films

SANS

Sprache
Englisch
Fachbereich/-gebiet
05 Fachbereich Physik > Institut für Physik Kondensierter Materie (IPKM)
DDC
500 Naturwissenschaften und Mathematik > 530 Physik
500 Naturwissenschaften und Mathematik > 540 Chemie
Institution
Universitäts- und Landesbibliothek Darmstadt
Ort
Darmstadt
Titel der Zeitschrift / Schriftenreihe
Applied Sciences
Jahrgang der Zeitschrift
11
Heftnummer der Zeitschrift
9
ISSN
2076-3417
Verlag
MDPI
Publikationsjahr der Erstveröffentlichung
2021
Verlags-DOI
10.3390/app11094036
PPN
485015188

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